Laboratório de Materiais Carbonosos e Cerâmicos / Laboratório de Plasma Térmico



  1. "Solid-state NMR spectroscopy of roasted and ground coffee samples: Evidences for phase heterogeneity and prospects of applications in food screening”, Jair. C. C. Freitas, Maria Ejaz, Alice T. Toci, Wanderson Romão, Yaroslav Z. Khimyak. Food Chemistry, 2023, 409:135317 (
  2. "Combined experimental and computational 1H NMR study of water adsorption onto graphenic materials", Alan R. Ambrozio, Thierry R. Lopes, Daniel F.Cipriano, Fábio A.L. de Souza, Wanderlã L. Scopel, Jair C.C.Freitas. Journal of Magnetic Resonance Open, 2023, 14-15: 100091 (
  3. "Grafted chitosan nanogel with 3,4-methylenedioxycinnamic acid: synthesis, characterization and application in the encapsulation of monoterpenes with antifungal properties", Giordane Ladeira, Stephanne Y. B. de Carvalho, Natália A. P. Rochaa, Isabela C. Soares, Daniel F. Cipriano, Jair C. C. Freitas, Luiz G. L. Guimarães. International Journal of Polymeric Materials and Polymeric Biomaterials, 2023. (
  4. "Inclusion complex of ketoconazole and p-sulfonic acid calix[6]arene improves antileishmanial activity and selectivity against Leishmania amazonensis and Leishmania infantum", Vagner T. de Queiroz, Bianca de O. Botelho, Natália A. Guedes, Diana C. Cubides-Román, Francisco de P. Careta, Jair C.C. Freitas, Daniel F. Cipriano, Adilson V. Costa, Ângelo de Fátima, Sergio A. Fernandes. International Journal of Pharmaceutics, 2023, 122663. (
  5. "Combined computational and experimental study about the incorporation of phosphorus into the structure of graphene oxide", Tainara L. G. Costa, Mariana A. Vieira, Gustavo R. Gonçalves, Daniel F. Cipriano, Valdemar Lacerda, Jr, Arlan S. Gonçalves, Wanderlã L. Scopel, Abner de Siervo, Jair C. C. Freitas. Physical Chemistry Chemical Physics, 2023, 25, 6927-6943.
  6.  "Phosphorus/Sulfur-Enriched Reduced Graphene Oxide Papers Obtained from Recycled Graphite: Solid-State NMR Characterization and Electrochemical Performance for Energy Storage", Mariana A. Vieira, Tainara L. G. Costa, Gustavo R. Gonçalves, Daniel F. Cipriano, Miguel A. Schettino, Jr., Elen L. da Silva, Andrés Cuña, Jair C. C. Freitas. C Journal of Carbon Research, 2023, 9, 60.
  7. "Fractal-like kinetics for enhanced boron adsorption on heterogeneous magnetic composite surfaces" Camila N. Pinotti, Juan A. Ramos-Guivar, José R.C. Proveti, Yamerson Canchanya-Huaman, Mayra-Alejandra Arias-Contreras, Noemi-Raquel Checca-Huaman, Daniel F. Cipriano, Eduardo P. Muniz, Honério C. Jesus, Dirk Baabe, Jair C.C. Freitas, F. Jochen Litterst, Edson C. Passamani. Materials Chemistry and Physics, 2023, 308, 128313.
  8. "Nanostructured faujasites with different structural and textural properties for adsorption of cobalt and nickel", Rodrigo S. Teixeira, Djanyna V. C. Schmidt, Fabiana S. dos Santos, Daniel F. Cipriano, Diêgo N. Faria, Jair C. C. Freitas, Mendelssolm K. Pietre. Brazilian Journal of Chemical Engineering, 2023,
  9. "Using 1H low-field NMR relaxometry to detect the amounts of Robusta and Arabica varieties in coffee blends", Rafael Oliari Muniz, Jorge L. Gonzalez, Aline T. Toci, Jair C. C. Freitas. Food Research International, 2023, 113610.
  10. "Effect of activated biochar as a low-cost catalyst on the quality of catalytic intermediate co-pyrolysis oil from waste polystyrene and green coconut pericarp." Heryson T.L. Arantes a, Marta A. Machado b, Mariana C. Santoro c, Jair C.C. Freitas c, Célia M. Ronconi d, Carolina B.P. Ligiero d, Sérvio T.A. Cassini e, Igor C.F. Sampaio f, Priscilla P. Luz. Fuel Processing Technology, 2023, 240, 107539.
  11. "Solid-state NMR for the analysis of interface excesses in Li-doped MgAl2O4 nanocrystals." André A. Bernardes, Andre L. da Silva, Jefferson Bettini, Jair C. C. Freitas, Ricardo H. R. Castro, Douglas Gouvêa. Journal of the American Ceramic Society. 2023, 1-14.
  12. "Valorization of pure poultry manure for biomass applications: Drying and energy potential characteristics." Vinícius Holanda Pasolini a, Ariany Binda Silva Costa a, Maisa Tonon Bitti Perazzini b, Daniel Fernandes Cipriano c, Jair Carlos Checon Freitas c, Hugo Perazzini b, Robson Costa Sousa. Renewable Energy. 2023. 119609.
  13. "Bridging Borophene and Metal Surfaces: Structural, Electronic, and Electron Transport Properties." Wanderlã L. Scopel, F. Crasto de Lima, Pedro H. Souza, José E. Padilha, and Roberto H. Miwa. The Journal of Physical Chemistry C. 2023, 127, 17556-17566.
  14. "A comprehensive study of the reduction of nitrate on natural FeTiO3: Photocatalysis and DFT calculations" Jefferson E. Silveira, Aramille S. de Souza, Fernando N.N. Pansini, Alyson R. Ribeiro, Wanderlã L. Scopel, Juan A. Zazo, Jose A. Casas, Wendel S. Paz.  Separation and Purification Technology. 2023, 306, 122570.


  1. "NMR spectral parameters of open- and closed-shell graphene nanoflakes: Orbital and hyperfine contributions”, F. A. L. de Souza, F. N. N. Pansini, L. F. Filho, A. R. Ambrozio, J. C. C. Freitas, W. L. Scopel. Carbon 2022;191:374-383 (
  2. “Crude dry extract from Colocasia esculenta in association with poly(vinyl alcohol) as biomaterial to prepare bioactive wound dressing”, E. M. L. de Prado, G. A. de Paula, J. A. P. Dutra, D. F. Cipriano, R. R. Kitagawa, F. D. M. Siman, E. F. Meira, J. C. C. Freitas, J. A. Severi, L. G. Carreira, R. L. Oréfice, J. C. O. Villanova. Polym. Bulletin 2022 (
  3. “Single step production of activated carbon from microalgae cultivated with urban wastewater”, R. N. Oss, R. F. Gonçalves, S. T. Cassini, M. A. Schettino Jr., D. F. Cipriano, J. C. C. Freitas. Algal Res. 2022;64:102669. (
  4. “Synthesis of nanostructured iron oxides and study of the thermal crystallization process using DSC and in situ XRD experiments”, L. M. Darabian, G. R. Gonçalves, M. A. Schettino Jr., E. C. Passamani, J. C. C. Freitas. Mater. Chem. Phys. 2022;285:126065 (
  5. “Fundamental studies on zeolite–adsorbate interactions: designing a better aluminosilicate adsorbent for pollutants’ removal”, M. K. de Pietre, J. C. C. Freitas. Environ. Earth Sci. 2022;81:17. (
  6. “A new magnetic composite with potential application in boron adsorption: Development, characterization, and removal tests”, C. N. Pinotti, L. M. de Souza, W. P. Marques, J. R. C. Provetti, H. C. Jesus, J. C. C. Freitas, P. S. S. Porto, E. P. Muniz, E. C. Passamani. Mater. Chem. Phys. 2022;277:125368 (
  7. VERBENO, C.H. ; PAES, V.Z.C. ; KROHLING, A.C. ; BUENO, T.E.P. ; GESHEV, J. ; VAN LIEROP, J. ; PASSAMANI, E.C. . Exchange bias and magnetic anisotropies in Co nanowire/IrMn film heterostructures. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, v. 546, p. 168768, 2022. (
  8. KROHLING, A.C. ; LEITE, H.D. ; FETTAR, F. ; MOSSANG, E. ; TONNERRE, J.M. ; MAGALHÃES-PANIAGO, R. ; BUENO, T. E. P. ; Passamani, E.C. ou Passamani, E. ; Nascimento, V.P. . Origin and properties of an unexpected exchange bias of Ta/Ni80Fe20/Ir20Mn80/Ta heterostructures in ultrathin limit: impact of the oblique deposition and Ta/Ni80Fe20 alloying. THIN SOLID FILMS, v. 746, p. 139115-139123, 2022. (
  10. SOUZA, EVERSON S. ; MENEZES, MARCOS G. ; SCOPEL, WANDERLÃ L. ; CAPAZ, RODRIGO B. . Spatially controlled graphene- lateral heterostructure for sensing applications: Insights from first-principles calculations. PHYSICAL REVIEW B, v. 105, p. 115413, 2022. (
  11. DE OLIVEIRA, IGOR S.S. ; DEUS, DOMINIKE P. DE A. ; SCOPEL, WANDERLÃ L. ; MIWA, ROBERTO H. . Tuning the electronic transport properties in few-layers GeP 3 intercalated by Cr-atoms. PHYSICA E-LOW-DIMENSIONAL SYSTEMS & NANOSTRUCTURES, v. xx, p. 115242, 2022. (
  12. PRETT, LUCAS CAMPAGNA ; VERISSIMO, MARCOS ; CARVALHO DE MELO RODRIGUES, DEBORA ; ALBUQUERQUE FILHO, MARCELO F. C. ; VENEZUELA, PEDRO ; SCOPEL, WANDERLA L. ; AMORIM, RODRIGO GARCIA . 2D GeP 3 and blue P: promising thermoelectric materials for room- and high-temperature applications. Materials Advances, v. 3, p. 4641, 2022. (
  13.  Synthesis of iron phosphide nanoparticles dispersed in activated carbon and their application in Fenton processes. G. R. Gonçalves, M. A. Schettino Jr., C. S. Schettino, V. Piccoli, H. C. de Jesus, M. A. Vieira, A. G. Cunha, J. C. C. Freitas. Journal of Nanoparticle Research, 2022; 24, 193.
  14. Use of Unmodified Coffee Husk Biochar and Ashes as Heterogeneous Catalysts in Biodiesel Synthesis. Joycel V. Fernández, Diêgo N. Faria, Mariana C. Santoro, Rafael Mantovaneli, Daniel F. Cipriano, Gilberto M. Brito, Maria Tereza W. D. Carneiro, Miguel A. Schettino Jr., Jorge L. Gonzalez, Jair C. C. Freitas. BioEnergy Research, 2022. 
  15. Synthesis of Graphene Quantum Dots by a Simple Hydrothermal Route Using Graphite Recycled from Spent Li-Ion Batteries. Lyane M. Darabian, Tainara L. G. Costa, Daniel F. Cipriano, Carlos W. Cremasco, Miguel A. Schettino, Jr., Jair C. C. Freitas. C-Journal of Carbon Research, 2022, 8, 48.


  1. “Synthesis of bilayer films from regenerated cellulose nanofibers and poly(globalide) for skin tissue engineering applications”, H. R. Amaral, J. A. Wilson, R. J. F. C. do Amaral, I. Pasçu, F. C. S. de Oliveira, C. J. Kearney, J. C. C. Freitas, A. Heise. Carbohydr. Polym. 2021;252:117201 (
  2. “Heterogeneous Fenton-like surface properties of oxygenated graphitic carbon nitride”, W. L. Oliveira, M. A. Ferreira, H. A. J. L. Mourão, M. J. M. Pires, V. Ferreira, H. F. Gorgulho, D. F. Cipriano, J. C. C. Freitas, V. R. Mastelaro, O. R. Nascimento, D. E. C. Ferreira, F. R. Fioravante, M. C. Pereira, J. P. de Mesquita. J. Colloid Interface Sci. 2021;587:479-488 (
  3. “Nanostructured faujasite zeolite as metal ion adsorbent: kinetics, equilibrium adsorption and metal recovery studies”, M. B. Goncalves, D. V. C. Schmidt, F. S. dos Santos, D. F. Cipriano, G. R. Gonçalves, J. C. C. Freitas, M. K. de Pietre. Water Sci. Technol. 2021;83:358-371 (
  4. “Reply to Comment on ‘On the difficulties and pitfalls with the analysis of solid-state 13C NMR spectra in graphitic materials’“, J. C. C. Freitas. Appl. Magn. Reson. 2021;52:91-98 (
  5. CUNHA, A.G.; CEVOLANI, M.B. ; CREMASCO, C.W. ; SCHETTINO, M.A. ; BUENO, T.E.P. ; EMMERICH, F.G. . An improved analyzer for measuring in-situ gas pressure in sealed quartz tube, and absolute and differential temperatures in heat treatments up to high temperatures. Journal of Instrumentation, v. 16, p. P07054, 2021. (
  6. OLIVEIRA, I. S. S. ; DEUS, D. P. A. ; OLIVEIRA, J. B. ; SCOPEL, W L ; MIWA, R. H. . Magnetic switch and electronic properties in chromium-intercalated two-dimensional GeP 3. PHYSICAL REVIEW MATERIALS, v. 5, p. 054002, 2021. (
  7. OLIVEIRA, D. WILSON ; SCOPEL, WANDERLÃ L. ; ALÍ, A. ; FONTES, M.B. ; SVANIDZE, E. ; MOROSAN, E. ; SAITOVITCH, E.B. ; GONZALEZ, J.L. . Theoretical study of the pressure effects on the electronic and magnetic properties of Sc3In. JOURNAL OF MAGNETISM AND MAGNETIC MATERIALS, v. 539, p. 168353, 2021. (
  8. PROCOPIO, ERIK F. ; N BATISTA, NATHANAEL ; L DE SOUZA, FÁBIO A. ; PAZ, WENDEL S. ; PALACIOS, JUAN JOSÉ ; SCOPEL, WANDERLÃ L. . Emergence of Topological Edge States in Oxidized α-In 2 Se 3 Nanosheets: Implications for Field-Effect Transistors. Acs Applied Nano Materials, v. 4, p. 8154-8161, 2021. (
  9. Gonzalez, J.L.. Multifractal statistic of porous structures simulated through fully penetrable sphere models. PHYSICA A-STATISTICAL MECHANICS AND ITS APPLICATIONS, v. 567, p. 125695, 2021. (
  10. PASCHOA, ANDERSON ; GONZALEZ, JORGE L. ; NASCIMENTO, VALBERTO P. ; PASSAMANI, EDSON C. . Extracting Stray Magnetic Fields from Thin Ferromagnetic Layers in Hybrid Superconducting/Ferromagnetic Heterostructures. Journal of Superconductivity and Novel Magnetism, v. 34, p. 3115-3124, 2021. (


  1. Increased arc length and stability in a magnetic gliding arc discharge using a cylindrical notched cathode.
  2. Designed single-phase ZrO2 nanocrystals obtained by solvothermal syntheses.
  3. Aproveitamento de precursores lignocelulósicos para produção de acetado de celulose.
  4. Production of Phosphorus-Containing Activated Carbons From Coffee Husk and Application in Adsorption Processes.
  5. Na,Ca-based catalysts supported on activated carbon for synthesis of biodiesel from soybean oil.
  6. Simulations of NMR Relaxation in a Real Porous Structure: Pre-asymptotic Behavior to the Localization Regime.
  7. Preparation of a Nitrogen Oil Compound Fraction by Modified Gel Silica Column Chromatography.
  8. Aplicação da RMN de 13C no estado sólido ao estudo dos teores de lignina e carboidratos em amostras de bagaço de cana submetidas a tratamento ácido.
  9.  13C NMR Parameters of Disordered Carbons: Atomistic Simulations, DFT Calculations, and Experimental Results. Journal of Physical Chemistry C.
  10. High-performance of activated biocarbon based on agricultural biomass waste applied for 2,4-D herbicide removing from water: Adsorption, kinetic and thermodynamic assessments.
  11. Study of thermal transformations in Na,Ca-based catalysts supported on activated carbon and their application in the synthesis of biodiesel from soybean oil.
  12. Eco-green biodiesel production from domestic waste cooking oil by transesterification using LiOH into basic catalysts mixtures.
  13. Potential and limitations of 13C CP/MAS NMR spectroscopy to determine the lignin content of lignocellulosic feedstock.
  14.  2,4-dichlorophenoxyacetic acid (2,4-D) micropollutant herbicide removing from water using granular and powdered activated carbons: a comparison applied for water treatment and health safety.
  15. Recycling of graphite and metals from spent Li-ion batteries aiming the production of graphene/CoO-based electrochemical sensors.
  16. Physicochemical characterization and in vitro biological evaluation of solid compounds from furazolidone-based cyclodextrins for use as leishmanicidal agents.
  17. Reply to Comment on -On the Difficulties and Pitfalls with the Analysis of Solid-State 13C NMR Spectra in Graphitic Materials.
  18. Nanostructured faujasite zeolite as metal ion adsorbent: kinetics, equilibrium adsorption and metal recovery studies.
  19. Tuning the Photocatalytic Water-Splitting Capability of Two-Dimensional α-In 2 Se 3 by Strain-Driven Band Gap Engineering for H 2 Production.
  20. Embedded carbon nanowire in black phosphorene and C-doping: the rule to control electronic properties.
  21. Electrically Sensing Hachimoji DNA nucleotides through a hybrid graphene/h-BN nanopore.
  22. Improved Removal Capacity and Equilibrium Time of Maghemite Nanoparticles Growth in Zeolite Type 5A for Pb(II) Adsorption.
  23. Two methods for solving electrostatic problems with azimuthal symmetry.
  24. Cobalt nanowire arrays grown on vicinal sapphire templates by DC magnetron sputtering.
  25. The influence of Cu spacer morphology in Cu/Py/Cu/Co/IrMn spin valves with induced non-collinear spin structures.
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